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Title: | A one pot synthesis of 5, 7-diaryl-1,5-dihydro (or 1, 2, 3, 5-tetrahydro)- pyrano[2, 3-d] pyrimidin-2, 4-diones (or 2-thioxo-4-ones) |
Authors: | Rahman, Md. Mahbubur Ahmed, S. Mosaddeq Siddiki, S. M. A. Hakim Halim, Md. Ershad Akhter, Kawsari Romman, U. K. R. Ahmed, M. Giasuddin |
Keywords: | Cyclocondensation, arylideneacetophenone, barbituric acid, phosphorous pentoxide |
Issue Date: | Jul-2013 |
Publisher: | University of Dhaka (DU) |
Series/Report no.: | 61(2);Page 167-171 |
Abstract: | A number of 5, 7-diaryl-1,5-dihydro (or 1, 2, 3, 5-tetrahydro)- pyrano[2, 3-d] pyrimidin-2, 4-diones (or 2-thioxo-4-ones) (3a-f) has been synthesized in one-step by the cyclocondensation of barbituric acid or thiobarbituric acid (1) with arylideneacetophenones (2a-c), in glacial acetic acid in the presence of phosphorous pentoxide. The structures of the compounds 3a-f have been determined by their UV, IR, 1H NMR, 13C NMR, mass spectral data and elemental analyses. |
URI: | http://dspace.aiub.edu:8080/jspui/handle/123456789/216 |
ISSN: | 1022-2502 |
Appears in Collections: | Publication: Journal |
Files in This Item:
File | Description | Size | Format | |
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Pyrano-4_DUJS_2013.docx | Summary Sheet | 4.07 MB | Microsoft Word XML | View/Open |
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